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High Resolution – Nuclear Magnetic Resonance (HR-NMR- 600) with Solid State facility

High Resolution – Nuclear Magnetic Resonance (HR-NMR- 600) with Solid State facility
 

Make: Bruker India Scientific
Model: Avance Neo 600 MHz

AVANCE NEO 600 MHz NMR Spectrometer

  • NMR Spectroscopy will be primarily used to determine the structure of known/unknown molecules in solution as well as in solid state.
  • It will also be used for the determination of purity and harmful components of various stuff of daily use such as foods, dyes, detergents, soaps, fats, oils and polymers.
  • Spectra can be obtained for most solids, e.g., Pharmaceuticals, Polymers, batteries, crystallography, glasses and biosolids. It will also help in characterizing new catalysts, membranes, proteins etc.
  • Fine spectroscopic technique to determine the molecular structure.
  • In addition to conventional solution state measurement this particular instrument can be used to determine the structure in solid state.
  • Solid state measurement can of tremendous help to pharmaceutical industries, electrochemistry and life sciences related studies.
  • Large variety of deuterated NMR solvents and state of the art analysis software are available for better spectra.
  • Experienced and well-trained personnel take care of the instruments.

Required Samples :-

5-10 mg of sample needed for 1H NMR

20-40 mg of sample needed for  13C NMR

Form Application :-

Click to Book Online

User Charges :-

  User Charges
Services Description / Analysis Type / Description Technology RUN TIME BHU & Start-Ups Other Academic Institution, R&D Labs, MSMEs Large Industrial Establishment

NMR based Experiments (Solvent Provided by Facility)

Experiments upto two hour(per 60min) 2D (COSY/HSQC/HMBC/NOESY)

Solvent : CDCl3, DMSO-d6 , D2O, Benzene-d6 , Methanol-d4 , Acetonitrile-d3 , THF-d8

*Solvent price for 1H is to be charged along with 2D charge


(Booking avilable in offline mode only.) 		60 MIN 700
1400
2800

Both 1H and 13C (Solvent Provided by User)

Both 1H and 13C (8-16 scans for 1H and, 256 scans for cryo probe, 512 scans for normal liquid probe for 13C)

 per sample 250 500 1000

Individual Measurment (Solvent Provided by User)

13C (256 scans for cryo probe, 512 scans for normal liquid probe), 11B, 19F, 31P Sample preference (15-25 mg)

 per sample 170 340 680

NMR based Experiments (Solvent Provided by User)

2D Experiments (per 60min) (COSY/HSQC/HMBC/NOESY)

 60 MIN 700 1400 2800

Individual Measurment (Solvent Provided by User)

1H (8-16 scans) Sample preference (3-8 mg)

 per sample 84 168 336

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : CDCl3

 per sample 150 300 600

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : DMSO-d6

 per sample 500 1000 2000

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : D2O

 per sample 350 700 1400

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : Benzen-d6

 per sample 450 900 1800

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : Methanol-d4

 per sample 1110 2220 4440

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : Acetonitrile-d3

 per sample 1080 2160 4320

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : THF-d8

 per sample 4060 8120 16420

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  CDCl3

 per sample 210 420 840

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  DMSO-d6

 per sample 570 1140 2280

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  D2O

 per sample 420 840 1680

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  Benzene-d6

 per sample 520 1040 2080

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  Methanol-d4

 per sample 1180 2360 4720

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  Acetonitrile-d3

 per sample 1150 2300 4600

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  THF-d8

 per sample 4130 8260 16520

NMR based Experiments : Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : CDCl3

 per sample 300 600 1200

NMR based Experiments : Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : DMSO-d6

 per sample 620 1240 2480

NMR based Experiments : Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : D2O

 per sample 470 940 1880

NMR based Experiments : Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : Benzene-d6

per sample 570 1140 2280

NMR based Experiments : Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : Methanol-d4

 per sample 1230 2460 4920

NMR based Experiments : Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : Acetonitrile-d3

 per sample 1200 2400 4800

NMR based Experiments : Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : THF-d8

 per sample 4180 8360 16720

NMR based Experiments (600 MHz Solid-State)

Experiments up to one-hour (per 60 min) 1D, 1H-13C, 15N Cross polarization (CP), 2D HETCOR

 60 MIN 1200 2400 4800

NMR based Experiments (600 MHz Solid-State)

Experiments longer than three hours* (Maximum 6 hours*)

 60 MIN 1000 2000 4000
Note :- 18% GST is applicable with user charges.

* Request of time slot for more than 3 hours will be confirmed by the concerned authority
* Sunday will be utilized for maintenance and other additional work
* Solvent price for 1H is to be charged along with 2D charge

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