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High Resolution – Nuclear Magnetic Resonance (HR-NMR- 600) with Solid State facility

High Resolution – Nuclear Magnetic Resonance (HR-NMR- 600) with Solid State facility
 

Make: Bruker India Scientific
Model: Avance Neo 600 MHz

AVANCE NEO 600 MHz NMR Spectrometer

  • NMR Spectroscopy will be primarily used to determine the structure of known/unknown molecules in solution as well as in solid state.
  • It will also be used for the determination of purity and harmful components of various stuff of daily use such as foods, dyes, detergents, soaps, fats, oils and polymers.
  • Spectra can be obtained for most solids, e.g., Pharmaceuticals, Polymers, batteries, crystallography, glasses and biosolids. It will also help in characterizing new catalysts, membranes, proteins etc.
  • Fine spectroscopic technique to determine the molecular structure.
  • In addition to conventional solution state measurement this particular instrument can be used to determine the structure in solid state.
  • Solid state measurement can of tremendous help to pharmaceutical industries, electrochemistry and life sciences related studies.
  • Large variety of deuterated NMR solvents and state of the art analysis software are available for better spectra.
  • Experienced and well-trained personnel take care of the instruments.

Required Samples :-

5-10 mg of sample needed for 1H NMR

20-40 mg of sample needed for  13C NMR

Form Application :-

Click to Book Online

User Charges :-

  User Charges
Services Description / Analysis Type / Description Technology RUN TIME BHU & Start-Ups Other Academic Institution, R&D Labs, MSMEs Large Industrial Establishment

NMR based Experiments (Solvent Provided by Facility)

Experiments upto two hour(per 60min) 2D (COSY/HSQC/HMBC/NOESY)

Solvent : Benzene-d6

 60 MIN 1000 2000 4000

Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : CDCl3

 per sample 240 480 960

Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : DMSO-d6

 per sample 620 1240 2480

Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : D2O

 per sample 470 940 1880

Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : Benzene-d6

per sample 570 1140 2280

Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : Methanol-d4

 per sample 1230 2460 4920

Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : Acetonitrile-d3

 per sample 1200 2400 4800

Both 1H and 13C (Solvent Provided by Facility)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

Solvent : THF-d8

 per sample 4180 8360 16720

NMR based Experiments (Solvent Provided by Facility)

Experiments upto two hour(per 60min) 2D (COSY/HSQC/HMBC/NOESY)

Solvent : CDCl3

 60 MIN 700 1400 2800

NMR based Experiments (Solvent Provided by Facility)

Experiments upto two hour(per 60min) 2D (COSY/HSQC/HMBC/NOESY)

Solvent : DMSO-d6

 60 MIN 1000 2000 4000

NMR based Experiments (Solvent Provided by Facility)

Experiments upto two hour(per 60min) 2D (COSY/HSQC/HMBC/NOESY)

Solvent : D2O

 60 MIN 1000 2000 4000

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  THF-d8

 per sample 4130 8260 16520

NMR based Experiments (Solvent Provided by Facility)

Experiments upto two hour(per 60min) 2D (COSY/HSQC/HMBC/NOESY)

Solvent : Methanol-d4

 60 MIN 1900 3800 7600

NMR based Experiments (Solvent Provided by Facility)

Experiments upto two hour(per 60min) 2D (COSY/HSQC/HMBC/NOESY)

Solvent : Acetonitrile-d3

 60 MIN 1900 3800 7600

NMR based Experiments (Solvent Provided by Facility)

Experiments upto two hour(per 60min) 2D (COSY/HSQC/HMBC/NOESY)

Solvent : THF-d8

 60 MIN 5000 10000 20000

NMR based Experiments (Solvent Provided by Facility)

Experiments longer than two hours*

Solvent : CDCl3


(Booking avilable in offline mode only.) 		60 MIN 750
Rs. 50+ Rs. 700/60 min upto two hours then Rs. 200/30 min for following hours (Maximum 3 hours*) 		1500
Rs. 100+ Rs. 1400/60 min upto two hours then Rs. 500/30 min for following hours (Maximum 3 hours*) 		3000
Rs. 200+ Rs. 2800/60 min upto two hours then Rs. 1000/30 min for following hours (Maximum 3 hours*)

NMR based Experiments (Solvent Provided by Facility)

Experiments longer than two hours*

Solvent : DMSO-d6


(Booking avilable in offline mode only.) 		60 MIN 1200
Rs. 200+ Rs. 1000/60 min upto two hours then Rs. 200/30 min for following hours (Maximum 3 hours*) 		2400
Rs. 400+ Rs. 2000/60 min upto two hours then Rs. 500/30 min for following hours (Maximum 3 hours*) 		4800
Rs. 800+ Rs. 4000/60 min upto two hours then Rs. 1000/30 min for following hours (Maximum 3 hours*)

NMR based Experiments (Solvent Provided by Facility)

Experiments longer than two hours*

Solvent : D2O


(Booking avilable in offline mode only.) 		60 MIN 1200
Rs. 200+ Rs. 1000/60 min upto two hours then Rs. 200/30 min for following hours (Maximum 3 hours*) 		2400
Rs. 400+ Rs. 2000/60 min upto two hours then Rs. 500/30 min for following hours (Maximum 3 hours*) 		4800
Rs. 800+ Rs. 4000/60 min upto two hours then Rs. 1000/30 min for following hours (Maximum 3 hours*)

NMR based Experiments (Solvent Provided by Facility)

Experiments longer than two hours*

Solvent : Benzene-d6


(Booking avilable in offline mode only.) 		60 MIN 1200
Rs. 200+ Rs. 1000/60 min upto two hours then Rs. 200/30 min for following hours (Maximum 3 hours*) 		2400
Rs. 400+ Rs. 2000/60 min upto two hours then Rs. 500/30 min for following hours (Maximum 3 hours*) 		4800
Rs. 800+ Rs. 4000/60 min upto two hours then Rs. 1000/30 min for following hours (Maximum 3 hours*)

NMR based Experiments (Solvent Provided by Facility)

Experiments longer than two hours*

Solvent : Methanol-d4


(Booking avilable in offline mode only.) 		60 MIN 2100
Rs. 200+ Rs. 1900/60 min upto two hours then Rs. 200/30 min for following hours (Maximum 3 hours*) 		4200
Rs. 400+ Rs. 3800/60 min upto two hours then Rs. 500/30 min for following hours (Maximum 3 hours*) 		8400
Rs. 800+ Rs. 7600/60 min upto two hours then Rs. 1000/30 min for following hours (Maximum 3 hours*)

NMR based Experiments (Solvent Provided by Facility)

Experiments longer than two hours*

Solvent : Acetonitrile-d3


(Booking avilable in offline mode only.) 		60 MIN 2100
Rs. 200+ Rs. 1900/60 min upto two hours then Rs. 200/30 min for following hours (Maximum 3 hours*) 		4200
Rs. 400+ Rs. 3800/60 min upto two hours then Rs. 500/30 min for following hours (Maximum 3 hours*) 		8400
Rs. 800+ Rs. 7600/60 min upto two hours then Rs. 1000/30 min for following hours (Maximum 3 hours*)

NMR based Experiments (Solvent Provided by Facility)

Experiments longer than two hours*

Solvent : THF-d8


(Booking avilable in offline mode only.) 		60 MIN 5200
Rs. 200+ Rs. 5000/60 min upto two hours then Rs. 200/30 min for following hours (Maximum 3 hours*) 		10400
Rs. 400+ Rs. 10000/60 min upto two hours then Rs. 500/30 min for following hours (Maximum 3 hours*) 		20800
Rs. 800+ Rs. 20000/60 min upto two hours then Rs. 1000/30 min for following hours (Maximum 3 hours*)

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  Acetonitrile-d3

 per sample 1150 2300 4600

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : DMSO-d6

 per sample 500 1000 2000

Both 1H and 13C (Solvent Provided by User)

Both 1H and 13C (8-16 scans for 1H and 256-512 scans for 13C)

 per sample 150 300 600

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : D2O

 per sample 350 700 1400

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : Benzen-d6

 per sample 450 900 1800

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : Methanol-d4

 per sample 1110 2220 4440

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : Acetonitrile-d3

 per sample 1080 2060 4120

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : THF-d8

 per sample 4060 8120 16240

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  CDCl3

 per sample 180 360 720

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  DMSO-d6

 per sample 570 1140 2280

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  D2O

 per sample 420 840 1680

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  Benzene-d6

 per sample 520 1040 2080

Individual Measurement (Solvent Provided by the Facility)

13C (256-512 scans),11B,19F,31P

Solvent :  Methanol-d4

 per sample 1180 2360 4720

Individual Measurment (Solvent Provided by User)

13C (256-512 scans), 11B, 19F, 31P Sample preference (15-25 mg for 256 scans, 8-15mg for 512 scans)

 per sample 120 240 480

NMR based Experiments (Solvent Provided by User)

Experiments up to two-hour (per 60 min) 2D (COSY/HSQC/ HMBC/ NOSEY)

 60 MIN 600 1200 2400

NMR based Experiments (Solvent Provided by User)

Experiments longer than two hours*


(Booking avilable in offline mode only.) 		60 MIN 600
Rs. 600/60 min up to two hours then Rs.200/30 min for following hours (Maximum 3 hours*) 		1200
Rs. 1200/60 min up to two hours then Rs.500/30 min for following hours (Maximum 3 hours*) 		2400
Rs. 2400/60 min up to two hours then Rs.1000/30 min for following hours (Maximum 3 hours*)

Individual Measurment (Solvent Provided by User)

1H (8-16 scans) Sample preference (3-8 mg)

 per sample 60 120 240

Individual Measurement (Solvent Provided by the Facility)

1H (8-16 scans)

Solvent : CDCl3

 per sample 120 240 480

NMR based Experiments (Solvent Provided by the Facility)

Experiments upto two hour (per 60 min, COSY/ HSQC/HMBC/ NOSEY)

Solvent : CDCl3

 60 MIN 700 1400 2800

NMR based Experiments (Solvent Provided by the Facility)

Experiments longer than two hour*

Solvent : CDCl3

 60 MIN 750 1500 3000

NMR based Experiments

Experiments up to one-hour (per 60 min) 1D, 1H-13C, 15N Cross polarization (CP), 2D HETCOR

 60 MIN 800 1600 3200

NMR based Experiments

Experiments longer than three hours* (Maximum 6 hours*)

 60 MIN 600 1200 2400
Note :- 18% GST is applicable with user charges.

* Request of time slot for more than 3 hours will be confirmed by the concerned authority
* Sunday will be utilized for maintenance and other additional work

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